Söllradl, Stefan; Lührs, Hanna; Révay, Zsolt; Kudejova, Petra; Canella, Lea; Türler, Andreas (2013). Increasing the dynamic range for the analysis of boron in PGAA. Journal of Radioanalytical and Nuclear Chemistry, 298(3), pp. 2069-2073. Berlin: Springer Netherlands 10.1007/S10967-013-2739-9
|
Text
Söllradl et al.pdf - Published Version Available under License Publisher holds Copyright. Download (406kB) | Preview |
Prompt gamma activation analysis (PGAA) is especially sensitive for elements with high neutron-capture cross sections, like boron, which can be detected down to a level of ng/g. However, if it is a major component, the high count rate from its signal will distort the spectra, making the evaluation difficult. A lead attenuator was introduced in front of the HPGe-detector to reduce low-energy gamma radiation and specifically the boron gamma rays reaching the detector, whose thickness was found to be optimal at 10 mm. Detection efficiencies with and without the lead attenuator were compared, and it was shown that the dynamic range of the PGAA technique was significantly increased. The method was verified with the analyses of stoichiometric compounds: TiB2, NiB, PVC, Alborex, and Alborite.
Item Type: |
Journal Article (Original Article) |
---|---|
Division/Institute: |
08 Faculty of Science > Department of Chemistry, Biochemistry and Pharmaceutical Sciences (DCBP) |
UniBE Contributor: |
Söllradl, Stefan, Türler, Andreas |
Subjects: |
500 Science > 570 Life sciences; biology 500 Science > 540 Chemistry |
ISSN: |
0236-5731 |
Publisher: |
Springer Netherlands |
Language: |
English |
Submitter: |
Franziska Bornhauser-Rufer |
Date Deposited: |
04 Apr 2014 20:33 |
Last Modified: |
05 Dec 2022 14:31 |
Publisher DOI: |
10.1007/S10967-013-2739-9 |
BORIS DOI: |
10.7892/boris.46197 |
URI: |
https://boris.unibe.ch/id/eprint/46197 |