Bigler, Peter; Gjuroski, Ilche; Chakif, Dib; Furrer, Julien (2024). A Versatile Broadband Attached Proton Test Experiment for Routine 13C Nuclear Magnetic Resonance Spectroscopy. Molecules, 29(4) MDPI 10.3390/molecules29040809
|
Text
molecules-29-00809-v3.pdf - Published Version Available under License Creative Commons: Attribution (CC-BY). Download (5MB) | Preview |
The proposed broadband attached proton test sequence allows the user to easily record 13C nuclear magnetic resonance multiplicity-edited and quaternary-carbon-only spectra. Compared to earlier attached proton test experiments, it preserves both a tolerance for wide ranges of one-bond-coupling constant values and the effective suppression of residual CHn signals in the quaternary-carbon-only spectra. The recording of edited spectra or quaternary-carbon-only spectra is made easy by a single, user-controllable constant. These attributes make the broadband attached proton test experiment attractive for the 13C analysis of small molecules, including spectral editing, particularly in high-throughput analysis laboratories.
Item Type: |
Journal Article (Original Article) |
|---|---|
Division/Institute: |
08 Faculty of Science > Department of Chemistry, Biochemistry and Pharmaceutical Sciences (DCBP) |
UniBE Contributor: |
Bigler, Peter, Gjuroski, Ilche, Chakif, Dib, Furrer, Julien |
Subjects: |
500 Science > 570 Life sciences; biology 500 Science > 540 Chemistry 000 Computer science, knowledge & systems |
ISSN: |
1420-3049 |
Publisher: |
MDPI |
Language: |
English |
Submitter: |
Pubmed Import |
Date Deposited: |
27 Feb 2024 13:14 |
Last Modified: |
07 Aug 2024 15:44 |
Publisher DOI: |
10.3390/molecules29040809 |
PubMed ID: |
38398560 |
Uncontrolled Keywords: |
13C 1H 1JCH-tolerance APT Cq-only NMR broadband APT |
BORIS DOI: |
10.48350/193229 |
URI: |
https://boris.unibe.ch/id/eprint/193229 |
Actions (login required)
 |
Edit item |